
Emulsion Specification and Comparison Analysis in Construction Industry
Understanding the importance of specifications in utilizing scrub seal effectively, and exploring the components, challenges, and comparisons with conventional chip seal emulsions. Key topics include subcommittee membership, material components, the reasoning behind specification adjustments, evaluation methods, and motivation for adopting new testing techniques.
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Presentation Transcript
Scrub Seal Update Scrub Seal Update Andrew Hanz Mathy Construction Emulsion Task Force Meeting Indianapolis, IN June 21, 2018
Subcommittee Membership Codrin Daranga Andy Clayton Hussain Bahia Ken Gryzbowski Jeff Schoger Kevin Carlson Katy Fleury
Why have a specification? Scrub seal is being used effectively throughout the US. All based on proprietary specifications. Universal specification o Reduces confusion o Promotes competition o Promotes innovation
Components of the Materials Spec Polymer Modified Rejuvenating Emulsion o Emulsion o Emulsion Residue o Rejuvenating Agent o Polymer Aggregate o Gradation o Quality Requirements
Why was the spec. pulled back? Emulsion Residue Properties Emulsion Residue Properties Polymer Identification Polymer Identification Original Proposed test was MSCR %R, 3.2kPa at 10C >55%. 1. Elastomeric Systems Test could not differentiate between PMAs and CRS-2. Test temperature too low and material too stiff. Solution: MSCR at 52 C and 0.1kPa 2. Non-Elastomeric Systems MSCR or other elasticity test does not identify polymer presence. Solution: TBD
Scrub Seal vs Conventional Chip Seal Emulsions Scrub Seal vs Conventional Chip Seal Emulsions MSCR DSR at 52 C %R 0.1 %R 3.2 Emulsion G*/sind delta 10 52 58 10 52 58 CMS-2P 2.86 77 75.5% 29.9% 19.4% 68.3% 8.7% 3.0% CRS-2 3.228 85.3 63.0% 4.2% -0.4% 61.1% 0.8% 0.0% CRS-2P 4.494 74.4 77.7% 48.7% 47.7% 69.8% 26.8% 14.0% HFRS-2 5.13 76.8 79.5% 61.8% 53.9% 72.3% 10.5% 3.4% HFRS-2P 5.228 66.8 86.4% 83.0% 80.7% 78.4% 59.7% 35.0%
Emulsion Specification Table - Elastomeric PMREa Grade Min Max Tests on residue from distillationd: Penetration, 4 C (39 F), 200 g, 60 s, 0.1 mm 40 Or G* at 4 C 10 rad/s, 1% strain at Elastic Recovery, 25C T301 OR MSCR Percent Recovery at 0.1 kPa, 52 C (50 F), % Ash Content, % Viscosity, 60 C (140 F), Pa S Or Jnr at 52 C TBD 50? 20 1 500 4.5?? D Residue preparation for testing may use the alternate methods, R 78, ASTM D7403, or ASTM D7944, so as not to negatively affect the properties of any polymer modifiers contained therein
Motivation for Changes Allow Old and New Test Methods o Old: Penetration, viscosity, elastic recovery o New: All DSR based Why? Testing Time and Effort o All residue approval tests could be conducted on one machine. o Use of moisture balance significantly reduces time.
Next Steps All scrub seal emulsions o Evaluate demulsibility requirements. Considering removing from specification or a very high maximum (i.e. 80%) Elastomeric Systems o Distribute data table and solicit test results using Old and New approaches. Non-elastomeric Systems o Evaluate NCHRP 9-50 approach for polymer identification.