Polymerization Studies: Macromonomer Synthesis and Homopolymerization Kinetics

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Explore the detailed processes of macromonomer synthesis and homopolymerization kinetics in polymer chemistry. Topics covered include various synthesis methods, copolymer synthesis studies, and self-assembly analysis, providing valuable insights into polymer science and technology.

  • Polymer Chemistry
  • Macromonomer Synthesis
  • Homopolymerization
  • Copolymer Synthesis
  • Self-Assembly
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  1. Overall Organization CRIPT End-to-End Test Papers Reference to Xia et al. brushes Xia et al. brushes Macromonomer Synthesis Homopolymerization Kinetics Copolymer Synthesis Studies of Self-Assembly

  2. Macromonomer Synthesis THF PMDETA CuBr PnBA Click coupling n-butyl acrylate ATRP Poly(n- butylacrylate) PnBA NB(PnBA)4.0k n-butyl acrylate azidification Methyl 2- bromopropionate PnBA NMR Norbornenyl alkyne Sodium azide dimethylformamide PnBA GPC THF PMDETA CuBr PtBA Click coupling t-butyl acrylate ATRP Poly(t- PtBA NB(PtBA)4.7k t-butyl acrylate azidification butylacrylate) Methyl 2- bromopropionate PtBA NMR Sodium azide Norbornenyl alkyne dimethylformamide PtBA GPC

  3. Macromonomer Synthesis THF PMDETA CuBr PS 2.2 Click coupling Styrene 2.2 ATRP PS2.2 NB(PS)2.2k styrene Poly(styrene) 2.2 azidification Methyl 2- bromopropionate PS 2.2 NMR Norbornenyl alkyne Sodium azide dimethylformamide PS 2.2 GPC D,L-lactide LA 4.7 ring- opening polymerization PLA 4.7 NMR NB alcohol NB(PLA)4.7k PLA 4.7 GPC stannous octoate

  4. Macromonomer Synthesis THF PMDETA CuBr PS 6.6 Click coupling Styrene 6.6 ATRP PS 6.6 azidification NB(PS)6.6k styrene Poly(styrene) 6.6 Methyl 2- bromopropionate PS 6.6 NMR Norbornenyl alkyne Sodium azide dimethylformamide PS 6.6 GPC D,L-lactide LA 7.0 ring- opening polymerization PLA 7.0 NMR NB alcohol NB(PLA)7.0k PLA 7.0 GPC stannous octoate

  5. Homopolymerization Kinetics Homopolymerization Kinetics PnBA4.0k NB(PnBA)4.0k PS2.2k homopolymerization NB(PS)2.2k homopolymerization Ru Catalyst 1 Ru Catalyst 1 PnBA4.0k kinetics PS2.2k kinetics Tetrahydrofuran Tetrahydrofuran PtBA4.7k PLA4.7k PLA200 hompolymer NB(PtBA)4.7k NB(PLA)4.7k homopolymerization homopolymerization Ru Catalyst 1 Ru Catalyst 1 PtBA4.7k kinetics PLA4.7k kinetics Tetrahydrofuran Tetrahydrofuran

  6. Homopolymerization Kinetics Homopolymerization Kinetics PS6.6k NB(PS)6.6k homopolymerization Ru Catalyst 1 PS6.6k kinetics Tetrahydrofuran PLA7.0k NB(PLA)7.0k homopolymerization Ru Catalyst 1 PLA7.0k kinetics Tetrahydrofuran

  7. Copolymer Synthesis 1 of 8 Copolymer Synthesis NB(PS)6.6k g-[PS40-b-PnBA70] copolymerization g-[PS40-b-PnBA70] NB(PnBA)4.0k Ru Catalyst 1 g-[PS40-b-PnBA70] GPC Tetrahydrofuran NB(PS)6.6k g-[PS40-r- PnBA200] g-[PS40-r-PnBA200] copolymerization NB(PnBA)4.0k g-[PS40-r- PnBA200] GPC Ru Catalyst 1 Tetrahydrofuran

  8. Copolymer Synthesis 2 of 8 Copolymer Synthesis NB(PtBA)4.7k g-[PtBA100-b- PnBA100] copolymerization g-[PtBA100-b- PnBA100] NB(PnBA)4.0k Ru Catalyst 1 g-[PtBA100-b-PnBA100] GPC Tetrahydrofuran NB(PtBA)4.7k g-[PtBA100-b- PnBA200] copolymerization g-[PtBA100-b- PnBA200] NB(PnBA)4.0k Ru Catalyst 1 g-[PtBA100-b-PnBA200] GPC Tetrahydrofuran

  9. Copolymer Synthesis 3 of 8 Copolymer Synthesis NB(PS)2.2k g-[PS50-b-PtBA50] copolymerization g-[PS50-b-PtBA50] NB(PtBA)4.7k Ru Catalyst 1 g-[PS50-b-PtBA50] GPC Tetrahydrofuran NB(PS)2.2k g-[PS100-b- PtBA100] g-[PS100-b-PtBA100] copolymerization NB(PtBA)4.7k Ru Catalyst 1 g-[PS100-b-PtBA100] GPC Tetrahydrofuran

  10. Copolymer Synthesis 4 of 8 Copolymer Synthesis NB(PLA)4.7k g-[PLA20-b- PnBA180] g-[PLA20-b-PnBA180] copolymerization NB(PnBA)4.0k Ru Catalyst 1 g-[PLA20-b-PnBA180] GPC Tetrahydrofuran NB(PLA)4.7k g-[PLA40-b- PnBA160] g-[PLA40-b-PnBA160] copolymerization NB(PnBA)4.0k Ru Catalyst 1 g-[PLA40-b-PnBA160] GPC Tetrahydrofuran

  11. Copolymer Synthesis 5 of 8 Copolymer Synthesis NB(PLA)4.7k g-[PLA100-b- PnBA100] copolymerization g-[PLA100-b- PnBA100] NB(PnBA)4.0k Ru Catalyst 1 g-[PLA100-b-PnBA100] GPC Tetrahydrofuran NB(PLA)4.7k g-[PLA200-b- PnBA200] copolymerization g-[PLA200-b- PnBA200] NB(PnBA)4.0k Ru Catalyst 1 g-[PLA200-b-PnBA200] GPC Tetrahydrofuran

  12. Copolymer Synthesis 6 of 8 Copolymer Synthesis NB(PLA)4.7k g-[PLA50-r- PnBA50] g-[PLA50-r-PnBA50] copolymerization NB(PnBA)4.0k Ru Catalyst 1 g-[PLA50-r-PnBA50] GPC Tetrahydrofuran NB(PLA)4.7k g-[PLA100-r- PnBA100] copolymerization g-[PLA100-r- PnBA100] NB(PnBA)4.0k Ru Catalyst 1 g-[PLA100-r-PnBA100] GPC Tetrahydrofuran

  13. Copolymer Synthesis 7 of 8 Copolymer Synthesis NB(PLA)4.7k g-[PLA200-r- PnBA200] copolymerization g-[PLA200-r- PnBA200] NB(PnBA)4.0k Ru Catalyst 1 g-[PLA200-r-PnBA200] GPC Tetrahydrofuran NB(PLA)4.7k g-[PLA160-r- PnBA40] g-[PLA160-r-PnBA40] copolymerization NB(PnBA)4.0k Ru Catalyst 1 g-[PLA160-r-PnBA40] GPC Tetrahydrofuran

  14. Copolymer Synthesis 8 of 8 Copolymer Synthesis NB(PLA)4.7k g-[PLA130-r- PnBA70] g-[PLA130-r-PnBA70] copolymerization NB(PnBA)4.0k Ru Catalyst 1 g-[PLA130-r-PnBA70] GPC Tetrahydrofuran

  15. Self-Assembly Studies of Self-Assembly g-[PLA20-b-PnBA180] SAXS g-[PLA20-b- PnBA180] g-[PLA130-r-PnBA70] SAXS g-[PLA130-r- PnBA70] g-[PLA20-b-PnBA180] DSC g-[PLA130-r-PnBA70] DSC g-[PLA40-b-PnBA160] SAXS g-[PLA40-b- PnBA160] g-[PLA40-b-PnBA160] DSC g-[PLA160-r-PnBA40] SAXS g-[PLA160-r- PnBA40] g-[PLA100-b-PnBA100] SAXS g-[PLA100-b- PnBA100] g-[PLA160-r-PnBA40] DSC g-[PLA100-b-PnBA100] DSC

  16. Self-Assembly Studies of Self-Assembly g-[PLA50-r-PnBA50] SAXS g-[PLA50-r- PnBA50] SAXS 1/I vs 1/T g-[PLA50-r- PnBA50] g-[PLA50-r-PnBA50] DSC g-[PLA50-r-PnBA50] AFM g-[PLA100-r- PnBA100] SAXS g-[PLA100-r- PnBA100] SAXS 1/I vs 1/T g-[PLA100-r- PnBA100] g-[PLA100-r- PnBA100] Single Mol. AFM g-[PLA100-r- PnBA100] DSC g-[PLA100-r- PnBA100] AFM

  17. Self-Assembly Studies of Self-Assembly g-[PLA200-r- PnBA200] SAXS g-[PLA200-r- PnBA200] SAXS 1/I vs 1/T g-[PLA200-r- PnBA200] g-[PLA200-r- PnBA200] DSC g-[PLA200-r- PnBA200] AFM g-[PLA100-r- PnBA100] Single Mol. AFM PLA200 hompolymer g-[PLA200-b- PnBA200] Image g-[PLA200-b- PnBA200]

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